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  Instruments              
   
    TEM   SEM   FIB   SPF

Transmission electron microscopes offer the opportunity to probe the crystal structure, defects, local chemistry, electronic structure and related information at a nanometer-or-less length scale. This allows one to view individual atoms in a specimen, allowing a person to identify grain boundaries and other imperfections in a specimen.
The EPIC facility houses two advanced transmission electron microscopes, along with a complete array of specimen preparation tools.

  Hitachi HD-2300A STEM
 
  • High brightness FEG operated at 80, 120 and 200 kV
  • Two X-ray EDS detectors make it most sensitive in the world
  • Secondary electron detector for SE imaging
  • Bright-field detector for phase contrast STEM imaging
  • Annular dark field detector for Z-contrast STEM imaging
  • Gatan Cryo-TEM holder and transfer system
  • Low-dose operation mode
  • Gatan Enfina EELS spectrometer (to be installed at the end of 2009)
  • Hitachi live CCD for nano-diffraction
  • High voltage cryo-SEM capability: secondary electron imaging is suitable for checking thick and frozen samples, like cells, tissues up to tens of micron
  • Gatan heating stage, up to 900 degree

 

 
  Hitachi H-8100
 
  • 200kV thermionic emission (W hairpin filament)
  • Large specimen tilt (+/- 45 degrees) pole piece
  • In situ specimen straining and deformation stage
  • CBED, nanodiffraction capabilities
  • Hollow-Cone Illumination
  • TV rate CCD camera
  • PGT X-Ray detector and analysis system

 Hitachi H8100 Manual
Click here, download the file Non-NU user application form

 
  Analytical Scanning Transmission Atomic Resolution
  (A STAR) electron microscope (JEOL JEM-2100F FAST TEM)
 
  • High brightness Schottky emitter operated at 200kV
  • BF/ADF STEM detectors, EDS system and EMISPEC system for atomic resolution Z-contrast imaging, sub-nanoscale resolution EDS and PEELS point analysis, and automated line scans and maps.
  • UTW x-ray detector
  • Gatan TV-rate CCD camera
  • Top-hat aperture to eliminate hard x-rays
  • Several side-entry specimen holders
  • Standard single and double-tilt holders
  • Low-Z(Be) holder for analytical x-ray microanalysis
 
  Related topics:  Specimen Preparation